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Routine Analysis
Particle Size Determination
Polymorph Screening
Method Development & Validation
Particle Analytical
Solid state for Pharmaceutical Industry
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Welcome to Particle Analytical
Our services
Method Development & Validation
Method development, particle size
Polymorph Screening
BET
Bulk and Tapped Density
Determination of density
Determination of refraction index
Differential Scanning Calorimetry DSC
Dissolution rate measurements (non-GMP)
Dynamic Light Scattering
Dynamic Vapor Sorption DVS
Flowability
FTIR
Hot Stage Microscopy (non-GMP)
Intrinsic Dissolution Rate (non-GMP)
Laser diffraction
Microscopy and digital image analysis
Particle counting
SEM (non-GMP)
Thermogravimetric Analysis, TGA
UV-VIS spectroscopy
X-Ray Diffraction – XRD
Quality
GMP accreditations
ICH requirements
Cases
Why and what
Crash course in Solid State Analysis
What is physical characterisation?
What is a polymorph?
What is the size of a particle?
High risk in later development or “do it now”?
Crystal transitions in real life
“Insignificant change” with significant effect
Chocolate as drug
New peaks appearing on XRD
The need for equipment made redundant
The water content was predictable
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